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Table 2 Combined results from TGA, NMR, ICP and argentometric titration for compounds 8–12

From: Characteristics and properties of nano-LiCoO2 synthesized by pre-organized single source precursors: Li-ion diffusivity, electrochemistry and biological assessment

Compound no—reagent Ligand eq. vs. Co eq. Solvent molecules per complex Free lithium (eq.) LiCl (eq.)
8—LiOtBu 3 4 (residual THF) 1 Li per Co 2 Li per Co
9—LiOtBu + LiOPh 1 + 2 (3) 4 1 Li per Co 2 Li per Co
10—LiOiPr 3 2 THF 1 Li per Co 2 Li per Co
11—LiOEt 6 4–5 THF 4 Li per Co 2 Li per Co
12—LiOMe 3 2 THF/2 MeOH 1 Li per Co 2 Li per Co